AssayIndex

AX-2026-041411

GHRP-6 · 2 mg declared · ChinaPeptides Co., Ltd. (QYAOBIO) · lot QYB-2602-X4422

PASSPURITY ONLY
Report ID
AX-2026-041411
Compound
GHRP-6
Compound class
Growth-hormone axis peptides
Supplier
QYB — ChinaPeptides Co., Ltd. (QYAOBIO)
Batch / lot
QYB-2602-X4422
Declared label claim
2mg
Laboratory
Kestrel Bioanalytical
Assay date
16 Jan 2026
Submitted
31 Jan 2026
Quarter
2026-Q1
Submitter
b.vukovic
Sample provenance
Buyer-sourced
Section 1

Results

Measured against the index acceptance specification for the growth-hormone axis peptides class. A specification is a decision the index made; a result is a measurement. See where each threshold came from.

ParameterMethodResultUnitIndex spec
PurityRP-HPLC, 15 min gradient, 214 nm99.18% area≥ 99.0PASS
Total impuritiesRP-HPLC, sum of reported peaks0.82% area≤ 1.0PASS
Largest single impurityRP-HPLC — des-Lys (−128 Da)0.31% area≤ 1.00PASS
Identitynot ordered on this submissionnot determinedrequired for VERIFIED statusNOT TESTED
Total peptide contentby difference from the gravimetric mass balance92.88%w/wNOT TESTED
Target-compound contenttotal peptide content × purity92.12%w/wNOT TESTED
Gross fill (as weighed)five-place balance, under nitrogen2.26mg2 mg declaredNOT TESTED
Recovered target peptidegross fill × target content2.082mg2 mg claimNOT TESTED
Recovery against label claimrecovered ÷ claim104.1%90.0 – 110.0PASS
Water contentKarl Fischer, coulometric, duplicate1.95%≤ 9.0PASS
Counter-ion (acetate)anion-exchange ion chromatography4.80%≤ 12.0PASS
Residual solvent + inorganic residueestimated — see /methods/residual-solvents-q3c/0.37%NOT TESTED
Endotoxinnot ordered on this submissionnot determined≤ 5.0NOT TESTED
Sterilitynot ordered on this submissionnot determinedno growthNOT TESTED
Appearancevisual, diffuse light, black and white backgroundOff-white lyophilised cake, intactwhite to off-white intact cakePASS
Reconstitution clarityreconstituted per submitter procedureClear after 90 s gentle swirling, no particulatesclear, no visible particulatesPASS
pH (reconstituted, 1 mg/mL)potentiometric, two-point calibration5.142.5 – 8.0PASS
Retention time (observed)RP-HPLC, 15 min gradient4.46min4.56 ± 0.25 (normalised)PASS
Peak asymmetry (10 % height)Ph. Eur. 2.2.460.970.80 – 1.50PASS
Plate count, main peakN = 5.54 (t/w½)²56,037≥ 20,000PASS
Resolution to nearest impurityvs [D-Trp]-epimer0.78no index criterionREPORTED
Section 2

Chromatogram and peak integration

The figure is drawn from the table. It is not an independent illustration — if a number in the table changed, the trace would change with it.

06186123731855924746 GHRP-64.46 min · 99.18 % 4.35 same trace · ×200 vertical expansion, baseline-corrected · main peak off-scale reporting threshold 0.05 % area 048121620 Retention time (min) Response (mAU)
Figure 1. RP-HPLC trace, 15 min gradient, 214 nm. Drawn from the peak-integration table below: peak positions are the reported retention times, peak areas are the reported area percentages, peak widths follow the reported plate count of 56,037, and skew follows the reported asymmetry factor of 0.97. Baseline noise is seeded from the report ID and is illustrative. The lower panel is the same trace at a stated vertical expansion with the slow gradient drift subtracted, because at full scale a 0.31 % impurity against a 99.18 % main peak is a line two pixels tall; the main peak runs off-scale there by design.
#PeakRTArea (µV·s)% areaΔ mass (Da)
1GHRP-6 — main peak4.464,820,45599.18
2des-Lys (−128 Da)4.3515,0670.31-128.095
3bis-oxidised Trp (+32 Da)4.1712,6370.26+31.990
4[D-Trp]-epimer4.406,8040.140.000
5oxidised Trp (+16 Da)4.295,3460.11+15.995
Closure check — purity + Σ impurities 100.00CLOSES

Reporting threshold 0.05 % area. Peaks below it are not reported and are therefore excluded from the total, which overstates purity by their sum — see peak integration.

Section 4

Gravimetric mass balance

Water, counter-ion, residual and total peptide content are exhaustive and mutually exclusive categories. They must account for 100 % of the cake mass. The index closes this to within 0.02 pp and the build asserts it.

ComponentDetermination%w/w of cake
WaterKarl Fischer1.95
Counter-ion (acetate)ion chromatography4.80
Residual solvent + inorganic residueestimated0.37
Total peptide contentby difference92.88
Total100.00 CLOSES

Supplier certificate, as declared

The supplier's own figures for this lot, beside the independent measurement. Divergence is assessed against the batch median, not against this single report — see rule AX-R05.

FigureSupplier COAThis reportIndex note
Purity (% area)99.6299.18divergence +0.29 pp vs batch median
Total impurities (% area)not stated0.82
Largest single impurity (% area)not stated0.31
Water (%)0.61.95
Counter-ion (%)not stated4.80
Peptide content (%w/w)not stated92.88
Endotoxin (EU/mg)not statednot determined
Method stated on certificateNOno method section — the result cannot be reconciled against any other
Section 5

Provenance and caveats

Where a sample came from changes the weight of the evidence. The index treats it as a first-class field.

Sample provenance
Buyer-sourced
Evidentiary weight
Strongest available evidence in this index.
Chain of custody
Retail purchase → third-party forwarder (18 d) → laboratory (courier, cold pack, 5 d) → assay.
Assay date
16 Jan 2026
Submitted to the index
31 Jan 2026
Laboratory
Kestrel Bioanalytical, Melbourne, Australia
Method basis
15 min gradient · unit-resolution MS
Verification status
PURITY ONLY
Section 6

Annotations 2

Signed technical comments from index contributors. Not a discussion forum — annotations question or contextualise the result, and the data team replies where a reply is warranted.

label_claim
A retail vial is also a test of the label. Declared claim 2 mg against what the gravimetry recovers is a question only a purchased vial can answer honestly.
multiple_compare
Restricting every supplier comparison to buyer-sourced records is the sensitivity analysis the scorecards publish. On the current dataset it changes no ordering that was not already inside measurement noise.
Section 7

Related records

Same batch — lot QYB-2602-X4422 n=6

ReportLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-041406QYB-2602-X4422Janoshik2026-Q199.321.68Buyer-sourced0PASS
AX-2026-041407QYB-2602-X4422Janoshik2026-Q199.481.80107.2Buyer-sourced0PASS
AX-2026-041408QYB-2602-X4422Medutest2026-Q199.181.36107.4Buyer-sourced1MARGINAL
AX-2026-041409QYB-2602-X4422Nordanalyt2026-Q199.341.61Buyer-sourced0PASS
AX-2026-041410QYB-2602-X4422Nordanalyt2026-Q199.391.99Buyer-sourced0PASS
Other recent GHRP-6 records in the index.
ReportSupplierLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-042012AMBAMB-2603-S5667Janoshik2026-Q399.375.9088.8Laboratory-retained1MARGINAL
AX-2026-042528HJHJ-2603-R5329VendorInvestigate2026-Q398.691.8795.8Buyer-sourced0FAIL
AX-2026-042015AMBAMB-2603-S5667Janoshik2026-Q399.546.4497.1Buyer-sourced0PASS
AX-2026-042526HJHJ-2603-R5329Medutest2026-Q399.373.06Laboratory-retained0PASS
AX-2026-042527HJHJ-2603-R5329VendorInvestigate2026-Q399.212.7793.2Buyer-sourced0PASS
AX-2026-042525HJHJ-2603-R5329Janoshik2026-Q399.523.2492.0Buyer-sourced0PASS
AX-2026-042013AMBAMB-2603-S5667Kestrel2026-Q399.935.75Buyer-sourced0PASS
AX-2026-042017AMBAMB-2603-S5667Medutest2026-Q399.766.4297.4Buyer-sourced0PASS
Other recent QYB records in the index.
ReportCompoundLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-041471PT-141 (Bremelanotide)QYB-2607-L4875Janoshik2026-Q399.723.75101.7Buyer-sourced0PASS
AX-2026-041377IpamorelinQYB-2605-H3558Nordanalyt2026-Q399.934.35Buyer-sourced0PASS
AX-2026-041427RetatrutideQYB-2604-B4920PeptideMeter2026-Q397.932.45101.7Buyer-sourced0PASS
AX-2026-041428RetatrutideQYB-2604-B4920Janoshik2026-Q398.353.20Laboratory-retained0PASS
AX-2026-041473PT-141 (Bremelanotide)QYB-2607-L4875PeptideMeter2026-Q399.583.7494.4Buyer-sourced0PASS
AX-2026-041472PT-141 (Bremelanotide)QYB-2607-L4875PeptideMeter2026-Q399.933.94Buyer-sourced0PASS
AX-2026-041429RetatrutideQYB-2604-B4920Medutest2026-Q398.532.6999.8Buyer-sourced1MARGINAL
AX-2026-041431RetatrutideQYB-2604-B4920Janoshik2026-Q398.632.3294.2Buyer-sourced0PASS