AssayIndex
Submitter and annotator

kf_titrand

Karl Fischer coulometry. Water content is the most ignored number on any certificate.

first seen 2024-Q29 records submitted46 annotations
Section 1

Contribution

Both submits records and annotates other people's.

Records submitted 9 n=9
Annotations 46 n=46
Median purity submitted 98.84% n=9
Suppliers covered 8 n=9
Section 2

Records submitted

A submitter chose to buy this material and to pay for this assay. That choice is the selection mechanism behind the whole index and it is not random.

ReportCompoundSupplierLotLabQuarterPurity %Water %Recovery %ProvenanceFlagsResult
AX-2026-041646SS-31 (Elamipretide)FGPFGP-2601-R8955Janoshik2026-Q298.273.4590.7Buyer-sourced1FAIL
AX-2026-042272SemaglutideTFCTFC-2602-H9925Nordanalyt2026-Q199.091.42Buyer-sourced0PASS
AX-2025-019358SemaglutideHYBHYB-2510-H6122PeptideMeter2025-Q498.905.17Buyer-sourced0PASS
AX-2025-019735SemaglutideHomopeptideHOMO-2505-V3835Janoshik2025-Q398.606.41Buyer-sourced0PASS
AX-2025-018851DihexaFGPFGP-2408-S8496PeptideMeter2025-Q199.336.5388.9Buyer-sourced1MARGINAL
AX-2025-020511MOTS-cSSASSA-2501-M6154Nordanalyt2025-Q198.112.87Buyer-sourced0PASS
AX-2024-005237GHRP-2WXTWXT-2404-N2537Medutest2024-Q399.035.76Supplier-supplied0PASS
AX-2024-005387RetatrutidePPGPPG-2311-F8058Janoshik2024-Q298.844.25Buyer-sourced0PASS
AX-2024-005340EpitalonSIGSIG-2308-5947Janoshik2024-Q198.659.0689.6Buyer-sourced1FAIL
SupplierRecordsMedian purity
FGP2n<3
TFC1n<3
HYB1n<3
Homopeptide1n<3
SSA1n<3
WXT1n<3
PPG1n<3
SIG1n<3
Section 3

Annotations

Signed technical comments on records. The index does not moderate annotations for agreement with its own arithmetic, and several of these disagree with it. Where a handle has made the same point on several records, one instance is shown and the rest are reachable from the records themselves.

AX-2026-043185
Water and content are coupled: a content figure on a dry basis and a water figure as-is cannot be added without converting one of them. The record states the basis for both.
AX-2026-041484
Water at 4.98 % is the largest non-peptide slot on most records and the one most often missing. Where it is present the balance can be closed; where it is not, nothing can.
AX-2026-041208
Where water is high and content was not measured, the recovered mass cannot be computed at all. Water alone bounds it from above and that bound is the only thing available.
AX-2026-041210
11.01 % water on NAD+, above the class specification. Water is the number that moves recovered mass per vial, and it is the one most often absent from a certificate entirely. Here it was measured, which is the reason anything can be said about it.
AX-2026-042707
Water at 4.70 % is the largest non-peptide slot on most records and the one most often missing. Where it is present the balance can be closed; where it is not, nothing can.
AX-2026-041211
10.94 % water on NAD+, above the class specification. Water is the number that moves recovered mass per vial, and it is the one most often absent from a certificate entirely. Here it was measured, which is the reason anything can be said about it.
AX-2026-041995
Water at 4.00 % is the largest non-peptide slot on most records and the one most often missing. Where it is present the balance can be closed; where it is not, nothing can.
AX-2026-042715
Nothing outstanding on this record. Balance closed, recovery computed, purity and identity both determined.
AX-2026-041855
Purity at 99.29 % and recovery at 89.8 % are independent findings. High purity and low recovery is a formulation and fill result, not a synthesis one.
AX-2026-043366
Water at 9.00 % is part of this. Remove it and the recovered figure moves by roughly the same amount, which is why water and content have to be read as a pair.
AX-2026-042547
Water at 2.00 % is the largest non-peptide slot on most records and the one most often missing. Where it is present the balance can be closed; where it is not, nothing can.
AX-2026-042862
Water at 8.08 % is the largest non-peptide slot on most records and the one most often missing. Where it is present the balance can be closed; where it is not, nothing can.

Showing 12 distinct comments of 46 annotations by this handle.